This paper reports the use of liquid chromatography/electrospray ionization tandem mass spectrometry (LC/ESI-MS/MS) method for the identification and quantification of residues of the natural insect control agent Spinosad in olive oils. The method determines the active ingredients Spinosyns A and D and two minor metabolites Spinosyns B and K without laborious sample treatment. All four analytes are determined simultaneously in a single injection using positive electrospray ionisation LC-MS with
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